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Paper ID:IJSREM68035

Prolonging the Initial Setting Time of Cement using Gypsum and Recycled Marble Powder for Hot Desert Climates

Stream/Area:

-

Subject:

-

Paper ID:

IJSREM68035

Volume:

10 |

10 |

Oct 2026

Pages:

1-5

Publication Frequency:

Monthly (12 issues per year)

DOI
Digital Object Identifier
10.55041/IJSREM68035

License:International Journal of Scientific Research in Engineering and Management follows the Creative Commons Attribution 4.0 (CC BY 4.0) License, allowing free use and distribution with proper attribution.

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Authors

N

Nevedika

Civil engineering

Sardar Beant Singh State University, Gurdaspur, Punjab, India

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Panav Dadwal

Panav Dadwal

Civil engineering

Sardar Beant Singh State University, Gurdaspur, Punjab, India

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Lovekesh

Lovekesh

Civil engineering

Sardar Beant Singh State University, Gurdaspur, Punjab, India

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Abstract

Concrete construction in hot desert environments (35◦C to 50◦C) faces significant technical hurdles due to accelerated cement hydration kinetics. Elevated temperatures trigger rapid tricalcium aluminate (C3A) dissolution, causing premature stiffening, flash set, and severe contraction of the Vicat initial setting time (IST) from a nominal 150 minutes down to under 45 minutes. This research investigates an optimized ternary binder system combining recalculated gypsum dosages (3.5–4.5% SO3) with Recycled Waste Marble Powder (WMP, 10–20% mass substitution) to regulate hydration heat release and restore placement open time. Isothermal microcalorimetry and Vicat penetration testing confirm that soluble sulfate from gypsum prevents early C3A flash setting, while fine calcite (CaCO3) from WMP stabilizes monocarboaluminate hydrates and dilutes C3S thermal output. The optimized ternary mix dampens peak heat release rates by 20–25% (3.4–3.9 mW/g) and successfully extends the IST to 120–145 minutes at 40◦C, providing a durable and sustainable solution for hot-weather concreting.

KEYWORDS

tricalcium aluminate (C3A) and tricalcium silicate (C3S) Portland pozzolona Cement (PPC)

Cite This Article

Nevedika, Panav Dadwal, Lovekesh, "Prolonging the Initial Setting Time of Cement using Gypsum and Recycled Marble Powder for Hot Desert Climates," International Journal of Scientific Research in Engineering and Management, vol. 10, no. 10, pp. 1-5, Oct 2026. https://doi.org/10.55041/IJSREM68035

Full Article/Conclusion

This study evaluated a practical, sustainable mineral intervention to overcome premature cement setting in hot desert environments. The key findings are summarized below: Desert Heat Impact: Temperatures above 35* accelerate cement hydration, cutting setting time to under 45 minutes. Gypsum Function: Adding 3%–4% gypsum provides soluble sulfate to prevent flash setting. Marble Powder Function: Waste Marble Powder (WMP) fills pore voids and forms monocarboaluminate to lower heat output.  Mix M1 (Control — 100% OPC): Initial setting time of 68 minutes due to unretarded clinker hydration.  Mix M2 (3% Gypsum / 5% WMP): Extended setting time to 92 minutes, but formed a weak, porous structure. Mix M3 (3% Gypsum / 7% WMP): Optimal blend — initial setting time of 88 minutes with the highest structural strength. Mix M_4 (4% Gypsum / 8% WMP): Longest setting time at 120 minutes, but suffered from water bleeding and poor matrix compatibility. Practical Outcome: The M3 blend (3% Gypsum + 7% WMP) restores placement open time while lowering cement carbon emissions by 12%–15%

References

1.               K. Scrivener, A. Ouzia, P. Juilland, and A. Kunhi Mohamed, “Advances in understanding hydration of Portland cement,” Cement and Concrete Research, vol. 124, p. 105823, 2019. 2.               S. Alonso, M. Palacios, and F. Puertas, “Comparative study of setting time and heat of hydration development of Portland cement according to EN 196-3,” IntechOpen Research Monographs, pp. 45–62, 2022. 3.               M. A. Gonzalez, R. Walker, and M. Sonebi, “Binary and ternary blends of construction and demolition waste and marble powder as supplementary cementitious materials,” MDPI Sustainability, vol. 17, no. 4, p. 1820, 2025. 4.               M. Fridrichova and K. Dvorak, “Heat evolution and mechanism of hydration in CaO–Al2O3–SO3 system,” Ceramics – Silikaty, vol. 49, no. 2, pp. 118–124, 2005

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Publication Date

10/17/2026

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Review Rounds: 2

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